1,8-二氮杂双环[5.4.0]十一碳-7-烯合成路线 （共 79 条）
反应条件
hydrogen bromide; bromine in acetic acid T=20 - 25°C; reagents: aq. HBr, NaBrO3;
参考文献
Muathen, Hussni A.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2740 - 2741
反应条件
in N,N-dimethyl-formamide
参考文献
Eisai Co., Ltd.
Patent: US5986088 A1, 1999 ;
参考文献
ICI Americas Inc.
Patent: US4975435 A1, 1990 ;
反应条件
in benzene 120°C; 2 h;;
参考文献
Riviere, P.; Castel, A.; Guyot, D.; Satge, J.
Journal of Organometallic Chemistry, 1985 , vol. 290, p. C15 - C18
反应条件
4-(N,N-dimethlyamino)pyridine; chloro-trimethyl-silane in tetrahydrofuran; ethyl acetate; 1,1'-carbonyldiimidazole; acetonitrile
参考文献
Thorarensen, Atli
Patent: US2002/143013 A1, 2002 ;
反应条件
in acetonitrile T=25°C; Darzens type reaction; Inert atmosphere;
参考文献
Demir, Ayhan S.; Emrullahoglu, Mustafa; Pirkin, Eser; Akca, Nazmiye
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 8992 - 8997
参考文献
API Corporation
Patent: EP1712630 A1, 2006 ;
参考文献
Ying, An-Guo; Chen, Xin-Zhi; Wu, Cheng-Lin; Zheng, Ren-Hua; Liang, Hua-Ding; Ge, Chang-Hua
Synthetic Communications, 2012 , vol. 42, # 23 p. 3455 - 3462
反应条件
in water; acetonitrile
参考文献
FMC Corporation
Patent: US4952580 A1, 1990 ;
参考文献
DOW CORNING CORPORATION; BACKER, Michael, Wolfgang; GOHNDRONE, John, Michael; KLEYER, Don, Lee; ZHOU, Xiaobing
Patent: WO2013/81820 A2, 2013 ;
Location in patent: Paragraph 0094 ;
