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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66895-45-2
合成路线
（共 13 条）
66895-34-9
→
反应条件
66895-45-2
反应条件
hydroxylamine hydrochloride; bentonite in ethanol 0.0666667 h; microwave irradiation;
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
66895-41-8
→
反应条件
66895-45-2
反应条件
1: With sodium hydroxide; bentonite in ethanol; water 0.0333333 h; microwave irradiation; 2: With acetic acid in ethanol; water
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
68667-54-9
→
反应条件
66895-45-2
反应条件
hydroxylamine hydrochloride in ethanol 0.0666667 h; microwave irradiation;
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
153381-58-9
+
67-64-1
丙酮
→
反应条件
66895-45-2
+
153335-51-4
反应条件
phosphorus pentoxide in N,N-dimethyl-formamide 24 h;
参考文献
Rashed, Nagwa; Hamid, Hamida Abdel; Ashry, El Sayed H. El
Carbohydrate Research, 1993 , vol. 243, # 2 p. 399 - 406
95-54-5
1,2-苯二胺
→
反应条件
66895-45-2
反应条件
1.1: 86 percent / acetic acid / ethanol; H2O / 0.07 h / microwave irradiation 2.1: 88 percent / bentonite / 0.12 h / microwave irradiation 3.1: bentonite; sodium hydroxide / ethanol; H2O / 0.03 h / microwave irradiation 3.2: 92 percent / acetic acid / ethanol; H2O View Scheme
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
100-63-0
苯肼
→
反应条件
66895-45-2
反应条件
1.1: 86 percent / acetic acid / ethanol; H2O / 0.07 h / microwave irradiation 2.1: 88 percent / bentonite / 0.12 h / microwave irradiation 3.1: bentonite; sodium hydroxide / ethanol; H2O / 0.03 h / microwave irradiation 3.2: 92 percent / acetic acid / ethanol; H2O View Scheme
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
50-81-7
抗坏血酸
→
反应条件
66895-45-2
反应条件
1: 86 percent / acetic acid / ethanol; H2O / 0.07 h / microwave irradiation 2: 95 percent / hydroxylamine hydrochloride; bentonite / ethanol / 0.07 h / microwave irradiation View Scheme
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
89-65-6
异抗坏血酸
→
反应条件
66895-45-2
反应条件
1: 86 percent / acetic acid / ethanol; H2O / 0.07 h / microwave irradiation 2: 76 percent / hydroxylamine hydrochloride / ethanol / 0.07 h / microwave irradiation View Scheme
参考文献
Ashry, El Sayed H. El; Atta, Kamal F.; Aboul-Ela, Salah; Beldi, Razika
Journal of Carbohydrate Chemistry, 2007 , vol. 26, # 1 p. 1 - 16
66895-50-9
→
反应条件
66895-45-2
反应条件
sodium hydroxide
参考文献
Henseke; Dittrich
Chemische Berichte, 1959 , vol. 92, p. 1550,1551
Full Text Show Details
Ashry et al.
Carbohydrate Research, 1978 , vol. 60, p. 303,312,313
153335-50-3
→
反应条件
66895-45-2
反应条件
acetic acid
参考文献
Rashed, Nagwa; Hamid, Hamida Abdel; Ashry, El Sayed H. El
Carbohydrate Research, 1993 , vol. 243, # 2 p. 399 - 406
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