反应条件
1.1: sec.-butyllithium / tetrahydrofuran / -93 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 0 °C 3.1: potassium phosphate / ethylene glycol dimethyl ether / 50 °C 4.1: potassium phosphate; Ni(PCy3)2Cl2 / toluene / 24 h / 110 °C / Inert atmosphere View Scheme
参考文献
Quasdorf, Kyle W.; Antoft-Finch, Aurora; Liu, Peng; Silberstein, Amanda L.; Komaromi, Anna; Blackburn, Tom; Ramgren, Stephen D.; Houk; Snieckus, Victor; Garg, Neil K.
Journal of the American Chemical Society, 2011 , vol. 133, # 16 p. 6352 - 6363