1-吗啉基-1-环己烯合成路线 (共 150 条)
反应条件
hydrogenchloride 1.) benzene, 20 min, 2.) 1 h; Yield given. Multistep reaction;
参考文献
Aizikovich, A. Ya.; Bazyl', I. T.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1203 - 1204
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1330 - 1332
反应条件
toluene-4-sulfonic acid in benzene 12 h; Heating;
参考文献
Farmaco, , vol. 52, # 1 p. 55 - 59
参考文献
Fos, Empar; Borras, Liset; Gasull, Maria; Mauleon, David; Carganico Germano
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 1 p. 203 - 208
反应条件
1: With 3H-2,1-benzoxaselenole Se-oxide; calcium sulfate; dihydrogen peroxide; potassium carbonate in methanol; dichloromethane T=20°C; 4 h; 2: With hydrogenchloride in water T=20°C; 2 h;
参考文献
Mercier, Eric A.; Smith, Chris D.; Parvez, Masood; Back, Thomas G.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3508 - 3517
反应条件
calcium sulfate; benzeneseleninic acid; dihydrogen peroxide in methanol; dichloromethane T=20°C;
参考文献
Mercier, Eric A.; Smith, Chris D.; Parvez, Masood; Back, Thomas G.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3508 - 3517
反应条件
hydrogenchloride; triethylamine in chloroform
参考文献
Science Union et Cie, Societe Francaise de Recherche Medicale
Patent: US4154851 A1, 1979 ;
反应条件
potassium permanganate on Y-Zeolite in 1,2-dichloro-ethane 6 h; Ambient temperature;
参考文献
Sreekumar; Padmakumar, Raghavakaimal
Tetrahedron Letters, 1997 , vol. 38, # 29 p. 5143 - 5146
反应条件
calcium sulfate; benzeneseleninic acid; dihydrogen peroxide in methanol; dichloromethane T=20°C;
参考文献
Mercier, Eric A.; Smith, Chris D.; Parvez, Masood; Back, Thomas G.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3508 - 3517
反应条件
water; magnesium bromide 1) ether, 15 h, r. t.; 2) 24 h; Yield given. Multistep reaction;
参考文献
Franck-Neumann, M.; Miesch, M.; Kempf, H.
Tetrahedron, 1988 , vol. 44, # 10 p. 2933 - 2942
反应条件
Yield given. Multistep reaction;
参考文献
Fisher, Gary B.; Goralski, Christian T.; Nicholson, Lawrence W.; Hasha, Dennis L.; Zakett, Donald; Singaram, Bakthan
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2026 - 2034