2-羟基-5-甲氧基苯甲醛合成路线 (共 150 条)
参考文献
Rubenstein
Journal of the Chemical Society, 1925 , vol. 127, p. 2003
反应条件
1-nitroethane; sodium acetate; acetic acid Reflux;
参考文献
Mulzer, Michael; Coates, Geoffrey W.
Organic Letters, 2011 , vol. 13, # 6 p. 1426 - 1428
反应条件
1: 79 percent / DABCO / 20 h / 50 °C 2: 92 percent / H2 / 10 percent Pd-C / methanol / 22 h / 2585.74 Torr / room t. 3: 76 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Viaud; Mamai; Guerin; Bennejean; Renard; Delagrange; Guardiola-Lemaitre; Howell; Guillaumet
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 1 p. 47 - 56
反应条件
potassium carbonate in acetone Williamson synthesis; 6 h; Reflux;
参考文献
Wempe, Michael F.; Jutabha, Promsuk; Quade, Bettina; Iwen, Timothy J.; Frick, Morin M.; Ross, Ian R.; Rice, Peter J.; Anzai, Naohiko; Endou, Hitoshi
Journal of Medicinal Chemistry, 2011 , vol. 54, # 8 p. 2701 - 2713
反应条件
potassium carbonate in acetone 6 h; Heating;
参考文献
Lamotte, Genevieve; Demerseman, Pierre; Royer, Rene
Synthesis, 1984 , # 12 p. 1068 - 1070
反应条件
potassium carbonate in acetone Substitution; Heating;
参考文献
Perez-Serrano, Leticia; Blanco-Urgoiti, Jaime; Casarrubios, Luis; Dominguez, Gema; Perez-Castells, Javier
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3513 - 3519
反应条件
1: potassium carbonate / dimethylformamide 2: acetic acide / Heating View Scheme
参考文献
Maillard; Langlois; Vo Van; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 4 p. 353 - 358
参考文献
Mukhanova; Kukushkin; Ivanov; Alekseeva; Granik
Russian Chemical Bulletin, 2007 , vol. 56, # 2 p. 325 - 329
反应条件
sodium acetate in acetic anhydride
反应条件
1: 2-hydroxy-5-methoxy-benzaldehyde With sodium methylate in anhydrous xylene T=60°C; 2 h; Inert atmosphere; 2: 2-triphenyl(α-carboxymethylene)phosphorane imidazolide in anhydrous xylene Intramolecular Wittig reaction; 48 h; RefluxInert atmosphere;
参考文献
Upadhyay, Puspesh K.; Kumar, Pradeep
Tetrahedron Letters, 2009 , vol. 50, # 2 p. 236 - 238