4-甲氧基-6-甲基-2H-吡喃酮合成路线 （共 57 条）
反应条件
magnesium methanolate in methanol
参考文献
Israili; Smissman
Journal of Organic Chemistry, 1976 , vol. 41, # 26 p. 4070 - 4074
反应条件
(i) iPrMgCl, PE, Et2O, (ii) /BRN= 115970/, THF; Multistep reaction;
参考文献
Stockinger,H.; Schmidt,U.
Justus Liebigs Annalen der Chemie, 1976 , p. 1617 - 1625
反应条件
5 Pd/Al2O3; hydrogen in isopropyl alcohol
T=20°C; P=1500.15 Torr;
参考文献
Schmidt, Erik; Bucher, Christoph; Santarossa, Gianluca; Mallat, Tamas; Gilmour, Ryan; Baiker, Alfons
Journal of Catalysis, 2012 , vol. 289, p. 238 - 248
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
1.5 h; Heatinglight irradiation;
参考文献
Evans, Nicholas R.; Devi, Lekshmi Sudha; Mak, Chris S. K.; Watkins, Scott E.; Pascu, Sofia I.; Koehler, Anna; Friend, Richard H.; Williams, Charlotte K.; Holmes, Andrew B.
Journal of the American Chemical Society, 2006 , vol. 128, # 20 p. 6647 - 6656
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane
2 h; HeatingIrradiationother solvent (benzene), reaction time, temperature, AIBN; Product distribution;
参考文献
Bacardit, R.; Moreno-Manas, M.; Pleixats, R.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 157 - 160
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
1.5 h; HeatingIrradiationother initiator (benzoyl peroxide), reaction time; Product distribution;
参考文献
Bacardit, R.; Moreno-Manas, M.; Pleixats, R.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 157 - 160
反应条件
1: selenium(IV) oxide / 1,4-dioxane / 5 h / 180 °C / Inert atmosphere; Sealed tube
2: n-butyllithium; triphenyl-methyl-phosphonium iodide / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere
3: sodium acetate; palladium diacetate / acetonitrile / 0.17 h
View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
