3,3-二甲基-1-苯基-2-丁酮合成路线 （共 50 条）
反应条件
tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide
T=0 - 10°C; electrolysis;
参考文献
d'Incan, Esther; Sibille, Soline; Perichon, Jacques; Moingeon, Marie-Odile; Chaussard, Jacques
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4175 - 4176
反应条件
potassium tert-butylate in ammonia
1 h; HeatingIrradiation;
参考文献
Semmelhack, M. F.; Bargar, Thomas
Journal of the American Chemical Society, 1980 , vol. 102, # 26 p. 7765 - 7774
反应条件
Diphenyliodonium fluoride in tetrahydrofuran
1) 37 min, -40 deg C 2) 1.8 h, to 6 deg C 3) 5.5 h, r.t.;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
potassium tert-butylate in ammonia
T=-76°C; 2.5 h; Irradiation;
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=25°C; 14 h; Irradiation;
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=25°C; 5 h; Irradiation; Further byproducts given;
参考文献
Cheng, Carlos; Stock, Leon M.
Journal of Organic Chemistry, 1991 , vol. 56, # 7 p. 2436 - 2443
反应条件
naphthalene; lithium
T=-78 - 0°C; Rearrangement; 1 h;
参考文献
Alonso, Emma; Guijarro, David; Martinez, Pedro; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1999 , vol. 55, # 36 p. 11027 - 11038
反应条件
1: 44 percent / sulfuric acid
2: 86 percent / tributyltin methoxide / dichlorobis(tri-o-tolylphosphine)palladium / toluene / 5 h / 100 °C
View Scheme
参考文献
Kosugi, Masanori; Hagiwara, Isao; Sumiya, Takao; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 241 - 246
反应条件
2,2-dimethylpropionamide
参考文献
House; Grubbs
Journal of the American Chemical Society, 1959 , vol. 81, p. 4733,4736
反应条件
2: 90 percent / EtONa / ethanol / 72 h / 50 °C
View Scheme
参考文献
Angle, Steven R.; Neitzel, Martin L.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6458 - 6461
