N-甲基-N-(2-吡啶)甲酰胺合成路线 （共 27 条）
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2.) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2.) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few mininutes 2.) reflux, 2 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2.) reflux, 3h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
1: C11H23N(15)N2O2SSi 2: N-methyl-N-(pyridin-2-yl)-formamide
参考文献
Geach, N. J.; Randall, G. P.; Winfield, C.J.
Journal of Labelled Compounds and Radiopharmaceuticals, 2004 , vol. 47, # 14 p. 1039 - 1040
反应条件
1.) tetrahydrofuran, 0 deg C, few minutes 2.) reflux, 3 h, THF, 65 deg C; Yield given. Multistep reaction;
参考文献
Comins, Daniel L.; Dernell, William
Tetrahedron Letters, 1981 , vol. 22, p. 1085 - 1088
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 25 min, 2.) THF, hexane, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wittenberger; Tasker; Sorensen; Donner
Synthetic Communications, 1993 , vol. 23, # 22 p. 3231 - 3248
