2-羟基-4-甲氧基苯甲醛合成路线 (共 227 条)
反应条件
piperidine in ethanol
4 h; Reflux;
参考文献
Kumar, B Vinay; Naik, Halehatty S. Bhojya; Girija; Kumar, B Vijaya
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 615 - 621
反应条件
piperidine in ethanol
Knoevenagel cyclization;
参考文献
Alizadeh, Abdolali; Ghanbaripour, Rashid; Zhu, Long-Guan
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-D0554-L, p. 2124 - 2126
反应条件
piperidine in methanol
T=20°C; Knoevenagel condensation;
参考文献
O'Callaghan, Conor N.; McMurry, T. Brian H.
Journal of Chemical Research, Miniprint, 1997 , # 3 p. 643 - 649
反应条件
bovine tendon hydrolysate in neat (no solvent)
T=55°C; 72 h; Green chemistry;
参考文献
Sangsuwan, Rapeepat; Sangher, Sasithorn; Aree, Thammarat; Mahidol, Chulabhorn; Ruchirawat, Somsak; Kittakoop, Prasat
RSC Advances, 2014 , vol. 4, # 26 p. 13708 - 13718
反应条件
analoge Reaktionen mit Benzoylessigsaeure-aethylester und mit Malonsaeure-diaethylester;
参考文献
Rangaswami; Seshadri; Venkateswarlu
Proceedings - Indian Academy of Sciences, Section A, 1941 , vol. 13, p. 316,318
反应条件
1: glacial acetic acid / 10 - 15 °C / Nitrierung
2: silver oxide; chloroform
View Scheme
参考文献
Rao; Srikantia; Iyengar
Journal of the Chemical Society, 1925 , vol. 127, p. 557
反应条件
1: 80 percent / K2CO3 / acetone / 1.5 h / Heating
2: 98 percent / NaH / tetrahydrofuran / 0.75 h / -30 °C
3: 81 percent / various solvent(s) / 4 h / Heating
4: 89 percent / mCPBA / CH2Cl2 / 0.5 h / 20 °C
View Scheme
参考文献
Guz, Nathan R; Lorenz, Peter; Stermitz, Frank R.
Tetrahedron Letters, 2001 , vol. 42, # 37 p. 6491 - 6494
反应条件
1: propionic acid-anhydride; piperidine
2: aqueous hydriodic acid
View Scheme
参考文献
Cingolani et al.
Gazzetta Chimica Italiana, 1953 , vol. 83, p. 647,651
反应条件
sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
T=20°C; Dakin reaction; 1 h;
参考文献
Bernet, Andreas; Seifert, Karlheinz
Helvetica Chimica Acta, 2006 , vol. 89, # 4 p. 784 - 796
反应条件
1: aniline / ethanol / 48 h / 20 °C
2: oxalyl chloride; pyridine / toluene
View Scheme
参考文献
Brunet, Ernesto; Garcia-Losada, Pablo; Rodriguez-Ubis, Juan-Carlos; Juanes, Olga
Canadian Journal of Chemistry, 2002 , vol. 80, # 2 p. 169 - 174