反,反,反-1,5,9-环十二烷基三烯合成路线 (共 41 条)
反应条件
in tetrahydrofuran; hexane T=-100°C; 1 h;
参考文献
Chemische Berichte, , vol. 118, # 6 p. 2330 - 2342
反应条件
diethylaluminium chloride; titanium tetrachloride in benzene T=60°C; 8 h; <6+2> cycloadditions with dienes and acetylenes catalyzed by titanium complexes, investigation of the complex of CHT with Ti(II)(AlCl4)2 and (η6-C6H6)Ti(II)(AlCl4)2;
参考文献
Tetrahedron, , vol. 40, # 17 p. 3295 - 3302
反应条件
diethylaluminium chloride; titanium tetrachloride Further byproducts given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 15 p. 805 - 806
反应条件
triethylaluminum; 2,2'-dipyridylmethane-Ni(OAc)2 in toluene T=80°C; 64 h; variation of catalyst, reaction temperature and time; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 335, p. 125 - 132
反应条件
copper 1.) ether 2.) 180 deg C, 20 Torr then 1 Torr;
参考文献
Tetrahedron, , vol. 42, # 6 p. 1711 - 1720
反应条件
in diethyl ether byproducts: N2; -80°C; instantaneous;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 699, p. 1 - 23
Ni: Org.Verb.2, 1.6.1.2, page 225 - 243
反应条件
bis(acetylacetonate)nickel(II); triethylaluminum; triphenylphosphine in benzene T=110°C; 6 h; other metal complexes; Product distribution;
参考文献
Russian Chemical Bulletin, , vol. 42, # 5 p. 872 - 878
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 916 - 921
反应条件
in benzene in 4 days; yellowish brown soln.; not isolated; identificated only with NMR;
参考文献
Diss. Bochum 1973, S. 1/95
反应条件
bis(acetylacetonate)nickel(II); monoethoxy-diethylaluminum T=35°C; other reagents; Rate constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 7 p. 1056 - 1062
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1509 - 1515
反应条件
in diethyl ether byproducts: N2, ((C6H5)2CN)2; -78°C heated cautiously to 20°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 699, p. 1 - 23
Ni: Org.Verb.2, 1.6.1.2, page 225 - 243