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in diethyl ether
(Ar); to soln. of Ti complex was added threefold excess of DCl in etherat -78°C, mixt. was slowly warmed up to room temp.; solvent was decanted and residue extd. with pentane, eytt. yielded CpTiCl3, residue was extd. with CH2Cl2, yielding Cp2TiCl2; identification by spectroscopy;
参考文献
Klei, E.; Teuben, J. H.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 97 - 108
in chloroform-d1
Irradiation (UV/VIS); UV photolysis in CDCl3-soln.;
参考文献
Kim, Jang Sub; Sen, Ayusman; Guzei, Ilia A.; Liable-Sands, Louise M.; Rheingold, Arnold L.
Journal of the Chemical Society. Dalton Transactions, 2002 , # 24 p. 4726 - 4731
Yu, Renyuan Pony; Darmon, Jonathan M.; Milsmann, Carsten; Margulieux, Grant W.; Stieber, S. Chantal E.; Debeer, Serena; Chirik, Paul J.
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