N,N-二甲基磷氨基二氯化物合成路线 （共 28 条）
参考文献
Pianka; Owen
Journal of Applied Chemistry, 1955 , vol. 5, p. 525,526
反应条件
NAF; benzene T=40 - 65°C;
参考文献
Schrader
Ang. Ch. Monogr., 1952 , vol. 62, p. 18
反应条件
1: 1-bromo-3,5-dimethyl-benzene With magnesium in tetrahydrofuran T=20°C; 2: N(Me)2P(O)Cl2 in tetrahydrofuran T=20°C; 3: With hydrogenchloride T=80°C; 1 h;
参考文献
Schroegel, Pamela; Hoping, Matthias; Kowalsky, Wolfgang; Hunze, Arvid; Wagenblast, Gerhard; Lennartz, Christian; Strohriegl, Peter
Chemistry of Materials, 2011 , vol. 23, # 22 p. 4947 - 4953
反应条件
diethyl ether; sodium
参考文献
Michaelis
Justus Liebigs Annalen der Chemie, 1903 , vol. 326, p. 172
反应条件
2,6-dimethylpyridine in benzene
参考文献
Revel,M.; Navech,J.
Bulletin de la Societe Chimique de France, 1973 , p. 1195 - 1200
参考文献
Skrowaczewska; Mastalerz
Roczniki Chemii, 1957 , vol. 31, p. 531,535
Chem.Abstr., 1958 , p. 2798
反应条件
triethylamine in benzene
参考文献
Ulrich,H. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1360 - 1362
反应条件
triethylamine in ethyl acetate
120 h; Ambient temperature;
参考文献
Holmes, Robert R.; Day, Roberta O.; Setzer, William N.; Sopchik, Alan E.; Bentrude, Wesley G.
Journal of the American Chemical Society, 1984 , vol. 106, # 8 p. 2353 - 2358
反应条件
(i) Et2O, (ii) NH3; Multistep reaction;
参考文献
Burg,A.B.; Slota,P.J.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2145 - 2148
反应条件
methanol; NAF; benzene
参考文献
Schrader
Ang.Ch.Monogr., 1952 , vol. 62, p. 21
