N-乙基-5-硝基吡啶-2-胺合成路线 （共 5 条）
反应条件
in dimethyl sulfoxide
5 h; Ambient temperature;
参考文献
Kijima, Atsushi; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3597 - 3602
反应条件
1: 89.1 percent / PCl5, POCl3 / 3 h / 110 °C
2: 71.1 percent / dimethylsulfoxide / 5 h / Ambient temperature
View Scheme
参考文献
Kijima, Atsushi; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3597 - 3602
反应条件
1: 51.2 percent / conc. H2SO4, NaNO2 / H2O / 0.5 h / 0 °C
2: 89.1 percent / PCl5, POCl3 / 3 h / 110 °C
3: 71.1 percent / dimethylsulfoxide / 5 h / Ambient temperature
View Scheme
参考文献
Kijima, Atsushi; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3597 - 3602
反应条件
in N,N-dimethyl-formamide
20 h; Heating;
参考文献
Bakke, Jan M.; Sletvold, Ingrid
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 15 p. 2710 - 2715
反应条件
sodium hydroxide in water
T=50°C; Kinetics;
参考文献
Kijima, Atsushi; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3597 - 3602
