反应条件
1: 1.) cuprous chloride / 1.) ether, -45 deg C, 10 min, 2.) ether, from -35 deg C to RT, 2 h
2: 86 percent / lithium chloride, water / dimethylsulfoxide / 14 h / Heating
3: 88 percent / lithium aluminium hydride
4: 75 percent / carbon tetrabromide, triphenylphosphine / CH2Cl2 / 12 h
View Scheme
参考文献
Beckwith, Athelstan L. J.; Easton, Christopher J.; Lawrence, Tony; Serelis, Algirdas K.
Australian Journal of Chemistry, 1983 , vol. 36, # 3 p. 545 - 556