in diethyl ether; water (under Ar, Schlenk); NaBH4 in water at 0°C deoxygenated by bubbling Ar for 30 min, soln. of (CH3(CH2)3)2SnCl2 in Et2O slowly added over 45 min, stirred for 15 min; sepd., washed with water, dried over MgSO4, concd. under vac.;
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Sawyer, A. K.; Brown, J. E.
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.7, page 62 - 63
in Petroleum ether byproducts: KCl; under N2, stirring equimolar amts. in petroleum ether at room temp. for3 h; filtn., washing with petroleum ether, combined filtrates are evapd., yellowish oil crystallizes at lower than room temp., elem. anal.;
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in dichloromethane; water soln. of Bu2SnCl2 in CH2Cl2 was added to deionized water and mixed vigorously until pH reached 1.3; org. layer sepd., dried over Na2SO4; evapd.; recrystallized from t-amyl alcohol; elem. anal.;
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H5PMo10V2O40 in acetonitrile T=70°C; Inert atmosphere; Solvent;
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