3,4-二甲基-3-戊烯-2-酮合成路线 （共 68 条）
反应条件
dihydrogen peroxide T=20°C; 24 h;
参考文献
Mokhtar, Hassan M.; Zaidlewicz, Marek
Polish Journal of Chemistry, 1981 , vol. 55, # 4 p. 757 - 761
反应条件
ozone in pentane T=-75°C;
参考文献
Griesbaum, Karl; Greunig, Hans-Joachim; Volpp, Willi; Jung, In-Chan
Chemische Berichte, 1991 , vol. 124, # 4 p. 947 - 956
反应条件
in methanol; dichloromethane Ambient temperature; Product distribution;
参考文献
Griesbaum, Karl; Zwick, Gerhard
Chemische Berichte, 1986 , vol. 119, # 1 p. 229 - 243
反应条件
1: magnesium; diethyl ether / beim Erhitzen des erhaltenen Alkohols mit Acetanhydrid und Natriumacetat 2: Raney nickel; methanol / 160 °C / 88260.9 Torr / Hydrogenation 3: palladium; methanol / 163 °C / 91202.9 Torr / Hydrogenation View Scheme
参考文献
Petrow; Melechin
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 1327,1330;engl.Ausg.S.1275,1277
反应条件
1: aq. HCl / methanol 2: NaOMe / bis-(2-methoxy-ethyl) ether / 159 °C 3: TCNE, O3 / methyl acetate / -60 °C View Scheme
参考文献
Stechl,H.-H.
Chemische Berichte, 1964 , vol. 97, p. 2681 - 2688
反应条件
ozone in dichloromethane T=-78°C; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 124, # 4 p. 947 - 956
反应条件
in methanol; dichloromethane Ambient temperature; Product distribution;
参考文献
Chemische Berichte, , vol. 119, # 1 p. 229 - 243
参考文献
PFW AROMA CHEMICALS B.V.
Patent: EP1184363 A1, 2002 ;
Location in patent: Example 2 ;
反应条件
ozone in pentane T=-75°C;
参考文献
Chemische Berichte, , vol. 124, # 4 p. 947 - 956
参考文献
Kondakow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1894 , vol. 26, p. 229
Full Text Show Details
Gheorghiu
Bull. Sect. Sci. Acad. Roum., vol. 8, p. 70
Chem. Zentralbl., 1923 , vol. 94, # III p. 209
