5,6-二甲基庚-5-烯-2-酮合成路线 （共 16 条）
参考文献
Kilby; Kipping
Journal of the Chemical Society, 1939 , p. 437
参考文献
Kilby; Kipping
Journal of the Chemical Society, 1939 , p. 437
反应条件
in ethanol; water
20 h; Ambient temperature;
参考文献
Mesnard; Miginiac; Fatome; et al.
European Journal of Medicinal Chemistry, 1980 , vol. 15, # 3 p. 247 - 252
反应条件
1: 1) NaH / 1) benzene, 1 h, r.t. 2) benzene, 0 deg C - r.t., 14 h
2: 56 percent / LiAlH4 / tetrahydrofuran / 0.5 h / 0 °C
3: 51 percent / Ph3P, CBr4 / acetonitrile / 3 h / 0 °C
View Scheme
参考文献
Okabe, Kazuaki; Muratake, Hideaki; Natsume, Mitsutaka
Tetrahedron, 1991 , vol. 47, # 40 p. 8559 - 8572
反应条件
diethyl ether; sodium amide
T=-15 - -10°C;
参考文献
Naves; Grampoloff; Bachmann
Helvetica Chimica Acta, 1947 , vol. 30, p. 1599,1609
参考文献
Kimel et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1611,1613
Full Text Show Details
Sarytschewa et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2662,2665; engl. Ausg. S. 2707, 2709
