5-溴-6-甲基-3-硝基-2-吡啶胺合成路线 （共 11 条）
反应条件
sulfuric acid; nitric acid
参考文献
Journal of the American Chemical Society, , vol. 79, p. 6421,6423,6424
反应条件
sulfuric acid; nitric acid T=0 - 60°C;
参考文献
Russian Journal of Applied Chemistry, , vol. 78, # 5 p. 787 - 790
反应条件
1: 25 g / Br2; AcONa; AcOH / 1 h / 15 °C 2: HNO3; H2SO4 / 0 - 60 °C View Scheme
参考文献
Russian Journal of Applied Chemistry, , vol. 78, # 5 p. 787 - 790
反应条件
sulfuric acid; sodium nitrite T=0°C; 0.5 h;
参考文献
Pomel; Rovera; Godard; Marsais; Queguiner
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1995 - 2005
反应条件
1: 80 percent / NaNO2, conc. H2SO4 / 0.5 h / 0 °C 2: 75 percent / POCl3, pyridine / chlorobenzene / 1 h / Heating 3: 90 percent / Et3N / 144 h / Heating View Scheme
参考文献
Pomel; Rovera; Godard; Marsais; Queguiner
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1995 - 2005
反应条件
1: SnCl2; aqueous HCl 2: aqueous HCl; NaNO2 3: palladium/charcoal; platinum; aq. NaOH solution / Hydrogenation View Scheme
参考文献
Graboyes; Day
Journal of the American Chemical Society, 1957 , vol. 79, p. 6421,6423,6424
反应条件
1: 90 percent / hydrazine hydrate; Zn / butan-1-ol / Heating 2: 90.5 percent / 4 h / 170 - 180 °C View Scheme
参考文献
Graboyes; Day
Journal of the American Chemical Society, 1957 , vol. 79, p. 6421,6423,6424
反应条件
1: 80 percent / NaNO2, conc. H2SO4 / 0.5 h / 0 °C 2: 75 percent / POCl3, pyridine / chlorobenzene / 1 h / Heating 3: 90 percent / Et3N / 144 h / Heating 4: 95 percent / H2 / 10percent Pd/C / ethanol / 760 Torr View Scheme
参考文献
Pomel; Rovera; Godard; Marsais; Queguiner
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1995 - 2005
反应条件
1: 80 percent / NaNO2, conc. H2SO4 / 0.5 h / 0 °C 2: 75 percent / POCl3, pyridine / chlorobenzene / 1 h / Heating View Scheme
参考文献
Pomel; Rovera; Godard; Marsais; Queguiner
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1995 - 2005
反应条件
1: SnCl2; aqueous HCl 2: aqueous HCl; NaNO2 View Scheme
参考文献
Graboyes; Day
Journal of the American Chemical Society, 1957 , vol. 79, p. 6421,6423,6424
