1,2,3,4-四氢-5-甲氧基咔唑合成路线 (共 7 条)
反应条件
1,8-diazabicyclo[5.4.0]undecane-4-ene; tert-butylhypochlorite in diethyl ether 1.) 0 deg C, 5 min, 2.) dimethylformamide, RT, 30 min;
参考文献
Kawase, Masami; Miyake, Yuko; Kikugawa, Yasuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1401 - 1404
反应条件
sodium acetate; acetic acid 4 h;
参考文献
WO2006/44232 A1, ;
Page/Page column 14; 16 ;
WO 2006/044232 A1
反应条件
toluene-4-sulfonic acid in ethanol Fischer indole synthesis; 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 71, # 20 p. 7899 - 7902
反应条件
N-chloro-succinimide; triethylamine in dichloromethane Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1401 - 1404
反应条件
methanol; potassium hydroxide; palladium on activated charcoal Hydrogenation;
参考文献
Journal of the Chemical Society, , p. 3475
反应条件
anschliessenden Erwaermen mit Essigsaeure;
参考文献
Journal of the Chemical Society, , p. 1115,1116
反应条件
T=110°C; other temperature; Rate constantKinetics;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 24, p. 154 - 158
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 24, # 2 p. 188 - 192