4-甲氧苯氧基乙醛二乙基缩醛合成路线 (共 6 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide 3 h; Heating;
参考文献
Bonini, Carlo; Cristiani, Graziella; Funicello, Maria; Viggiani, Licia
Synthetic Communications, 2006 , vol. 36, # 14 p. 1983 - 1990
参考文献
Justus Liebigs Annalen der Chemie, , vol. 312, p. 332
反应条件
1: 35 percent / poliphosphoric acid / benzene / 2 h / 100 °C 2: 80 percent / BBr3*SMe2 / chlorobenzene / 12 h / 130 °C 3: 60 percent / sodium hydride / dioxane / 6 h / 100 °C 4: 60 percent / sodium hydride / dimethylformamide / 3 h / 150 °C 5: 75 percent / aq.HCl / 2 h View Scheme
参考文献
Bonini, Carlo; Cristiani, Graziella; Funicello, Maria; Viggiani, Licia
Synthetic Communications, 2006 , vol. 36, # 14 p. 1983 - 1990
反应条件
1: 35 percent / poliphosphoric acid / benzene / 2 h / 100 °C 2: 80 percent / BBr3*SMe2 / chlorobenzene / 12 h / 130 °C View Scheme
参考文献
Bonini, Carlo; Cristiani, Graziella; Funicello, Maria; Viggiani, Licia
Synthetic Communications, 2006 , vol. 36, # 14 p. 1983 - 1990
反应条件
PPA in benzene 2 h; Heating;
参考文献
Barker, Peter; Finke, Paul; Thompson, Kevan
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 257 - 266
反应条件
hydrogenchloride in water; acetone
2 h; Heating / reflux;
参考文献
INCYTE CORPORATION; ZHUO, Jincong; METCALF, Brian
Patent: WO2008/64157 A1, 2008 ;
Location in patent: Page/Page column 51 ;