2,4,6-三溴-3-硝基苯酚合成路线 （共 11 条）
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide; calcium carbonate in methanol; dichloromethane
参考文献
Kakinami; Suenaga; Yamaguchi; Okamoto; Kajigaeshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3373 - 3375
反应条件
1: With β-cyclodextrin
12 h;
2: With bromine in tetrachloromethane
T=20°C; 24 h; Further stages. Further byproducts.;
参考文献
Suresh, Palaniswamy; Annalakshmi, Subramanian; Pitchumani, Kasi
Tetrahedron, 2007 , vol. 63, # 23 p. 4959 - 4967
反应条件
2: glacial acetic acid; bromine / Behandeln des Rohprodukts mit Wasser
View Scheme
参考文献
Bamberger
Chemische Berichte, 1915 , vol. 48, p. 1356
Chemische Berichte, 1916 , vol. 49, p. 1257
反应条件
hydrogen bromide; acetic acid
参考文献
Kohn; Segel
Monatshefte fuer Chemie, 1930 , vol. 56, p. 669
参考文献
Jackson; Koch
American Chemical Journal, 1899 , vol. 21, p. 519
反应条件
1: HNO3 / 100 °C
2: 100 °C
View Scheme
参考文献
Fox; Turner
Journal of the Chemical Society, 1930 , p. 1853,1860
反应条件
T=50 - 60°C; verduennen mit Wasser und Behandeln der Loesung mit Brom;
参考文献
Datta; Bhoumik
Journal of the American Chemical Society, 1921 , vol. 43, p. 311
参考文献
Fox; Turner
Journal of the Chemical Society, 1930 , p. 1853,1860
参考文献
Lindner
Chemische Berichte, 1885 , vol. 18, p. 612
参考文献
Jackson; Warren
American Chemical Journal, 1891 , vol. 13, p. 184
American Chemical Journal, 1893 , vol. 15, p. 618
Full Text Show Details
Jackson; Koch
American Chemical Journal, 1899 , vol. 21, p. 519
