二(仲-丁基)汞(II)合成路线 (共 15 条)
反应条件
in acetone
Kinetics; at 25°C;;
参考文献
Gmelin Handbook: Hg: MVol.B2, 182, page 781 - 784
反应条件
tetrabutylammomium bromide; oxygen in benzene
5 h; Ambient temperature; Yields of byproduct given;
参考文献
Uglova, E. V.; Reutov, O. A.
Doklady Chemistry, 1981 , vol. 257, p. 136 - 137
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 257, # 4 p. 896 - 897
反应条件
hydrogenchloride; ethanol; water
参考文献
Marker; Calvery
Journal of the American Chemical Society, 1923 , vol. 45, p. 820,822
反应条件
potassium bromide in nitromethane
byproducts: Ph2CH2, Ph2CH(sec-Bu); Ar atmosphere and absence of light and moisture; addn. of AgBF4 in nitromethane to soln. of alkylmercury, portionwise addn. of Ph2CHCl in nitromethane (20°C, TLC monitoring), washing with soln. of KBr; TLC;
参考文献
Uglova, E. V.; Petrovskii, K. B.; Fadeeva, S. S.; Mikhura, I. V.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1382 - 1386
反应条件
in acetonitrile
T=20°C; Yields of byproduct given;
参考文献
Uglova, E. V.; Petrovskii, K. B.; Fadeeva, S. S.; Mikhura, I. V.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1231 - 1234
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1382 - 1386