4-甲氧基环己-3-烯-1-醇合成路线 （共 11 条）
反应条件
ammonia; lithium in diethyl ether; ethanol T=-33°C; Birch reduction; 6 h;
参考文献
Suennemann, Hans Wolf; Hofmeister, Anja; Magull, Joerg; De Meijere, Armin
Chemistry - A European Journal, 2007 , vol. 13, # 13 p. 3739 - 3756
反应条件
hydrogen; 1-n-butyl-3-methylimidazolium tetrafluoroborate; Rh nanoparticles stabilized by poly(NVP-co-VBIMCl) T=75°C; P=30402 Torr; 12 h; Product distribution;
参考文献
Journal of Catalysis, , vol. 250, # 1 p. 33 - 40
反应条件
hydrogenchloride in chloroform 4 h; Ambient temperature; Yield given;
参考文献
Bell, Vivien L.; Holmes, Andrew B.
Synthetic Communications, 1982 , vol. 12, # 4 p. 323 - 326
反应条件
1: 82 percent / 1 M HCl / 0.75 h / 50 °C 2: 83 percent / imidazole / dimethylformamide / 5 h / Ambient temperature View Scheme
参考文献
Okamura, William H.; Elnager, Hassan Y.; Ruther, Michael; Dobreff, Susanne
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 600 - 610
反应条件
1: 90 percent / TosOH / benzene / Heating 2: 93 percent / NaH / tetrahydrofuran / Heating 3: 75 percent / 2 M aq. H2SO4 / acetone / Heating View Scheme
参考文献
Hwu; Leopold
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 11, p. 721 - 723
反应条件
hydrogenchloride T=50°C; 0.75 h;
参考文献
Okamura, William H.; Elnager, Hassan Y.; Ruther, Michael; Dobreff, Susanne
Journal of Organic Chemistry, 1993 , vol. 58, # 3 p. 600 - 610
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Hwu; Leopold
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 11, p. 721 - 723
反应条件
1: 90 percent / TosOH / benzene / Heating
2: 93 percent / NaH / tetrahydrofuran / Heating
3: 75 percent / 2 M aq. H2SO4 / acetone / Heating
4: 98 percent / HCl / ethanol / Heating
5: 85 percent / diethyl ether / Ambient temperature
6: DBU / tetrahydrofuran / 4 h / -5 °C
7: diethyl ether / -78 °C
View Scheme
参考文献
Hwu; Leopold
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 11, p. 721 - 723
反应条件
1: 90 percent / TosOH / benzene / Heating
2: 93 percent / NaH / tetrahydrofuran / Heating
View Scheme
参考文献
Hwu; Leopold
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 11, p. 721 - 723
反应条件
1: HCl / CHCl3 / 4 h / Ambient temperature
2: 43 percent / pyridinium dichromate / dimethylformamide / 6 h / 0 °C
View Scheme
参考文献
Bell, Vivien L.; Holmes, Andrew B.
Synthetic Communications, 1982 , vol. 12, # 4 p. 323 - 326
