双(乙酸根合-O)(3-甲氧)碘合成路线 (共 7 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane; acetonitrile T=-50°C; 2 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 18, # 39 p. 12232 - 12236
反应条件
boron trifluoride diethyl etherate in dichloromethane; acetonitrile T=-50°C; 2 h; Inert atmosphere;
参考文献
Khatri, Hem Raj; Zhu, Jianglong
Chemistry - A European Journal, 2012 , vol. 18, # 39 p. 12232 - 12236
反应条件
sodium periodate; sodium acetate in acetic acid
2 h; Heating;
参考文献
Zielinska, Agnieszka; Skulski, Lech
Molecules, 2002 , vol. 7, # 11 p. 806 - 809
反应条件
in acetic acid
T=-10 - 20°C;
参考文献
Chun, Joong-Hyun; Lu, Shuiyu; Pike, Victor W.
European Journal of Organic Chemistry, 2011 , # 23 p. 4439 - 4447
反应条件
sodium perborate; trifluorormethanesulfonic acid
T=40 - 45°C; 4 h;
参考文献
Hossain, Md. Delwar; Kitamura, Tsugio
Journal of Organic Chemistry, 2005 , vol. 70, # 17 p. 6984 - 6986
反应条件
1: I2, AgO2CCF3 / CH2Cl2
2: acetic acid
View Scheme
参考文献
Shah, A.; Widdowson, D. A.; Pike, V. W.
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 40, p. 65 - 67
参考文献
White; Caravatti; Kline; et al.
Tetrahedron, 1983 , vol. 39, # 14 p. 2393 - 2397