N-甲氧基-N-甲基苯甲酰胺合成路线 （共 140 条）
反应条件
1: benzoic acid With triethylamine; trichloromethyl chloroformate in dichloromethane T=0°C; 2: O,N-dimethyl-hydroxylamine hydrochloride in dichloromethane T=25°C; 1 h;
参考文献
Kim, Misoo; Lee, Hagyoung; Han, Ki-Jong; Kay, Kwang-Yol
Synthetic Communications, 2003 , vol. 33, # 23 p. 4013 - 4018
反应条件
pyridine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Fukushima, Naoki; Ieda, Naoya; Sasakura, Kiyoshi; Nagano, Tetsuo; Hanaoka, Kenjiro; Suzuki, Takayoshi; Miyata, Naoki; Nakagawa, Hidehiko
Chemical Communications, 2014 , vol. 50, # 5 p. 587 - 589
反应条件
potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether in toluene T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
反应条件
potassium phosphate in N,N-dimethyl-formamide T=80°C; 5 h; Inert atmosphere;
参考文献
Ueda, Tsuyoshi; Konishi, Hideyuki; Manabe, Kei
Organic Letters, 2012 , vol. 14, # 20 p. 5370 - 5373,4
反应条件
triethylamine; Sm(OTf)3 in tetrahydrofuran T=20°C; 72 h;
参考文献
Sibi, Mukund P.; Hasegawa, Hikaru; Ghorpade, Sandeep R.
Organic Letters, 2002 , vol. 4, # 20 p. 3343 - 3346
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=50°C; P=45004.5 Torr; 20 h; Autoclave; chemoselective reaction;
参考文献
Takacs, Attila; Petz, Andrea; Kollar, Laszlo
Tetrahedron, 2010 , vol. 66, # 25 p. 4479 - 4483
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
反应条件
1: O,N-dimethyl-hydroxylamine hydrochloride With sodium hydride T=22°C; 0.416667 h; 2: benzoic acid methyl ester in tetrahydrofuran T=130°C; 0.166667 h; microwave irradiation; Further stages.;
参考文献
Glynn, Daniel; Bernier, David; Woodward, Simon
Tetrahedron Letters, 2008 , vol. 49, # 39 p. 5687 - 5688
反应条件
n-butyllithium in tetrahydrofuran T=-20 - 20°C; Substitution; 2 h;
参考文献
Raap, Jan; Nieuwenhuis, Saskia; Creemers, Alain; Hexspoor, Sander; Kragl, Udo; Lugtenburg, Johan
European Journal of Organic Chemistry, 1999 , # 10 p. 2609 - 2621
反应条件
1: benzoic acid With methanesulfonyl chloride; triethylamine in tetrahydrofuran T=0°C; 0.166667 h; 2: N,O-dimethyl-hydroxylamine in tetrahydrofuran T=0°C; 1 h;
参考文献
Woo, Jacqueline C. S.; Fenster, Erik; Dake, Gregory R.
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8984 - 8986
