反式-2,5-二甲基-3-己烯合成路线 (共 20 条)
反应条件
o-xylene Irradiationother energy triplet sensitizers and other solvents, isomerization, photostationary ratios <E/Z>pss; Product distribution;
参考文献
Snyder, John J.; Tise, Frank P.; Davis, Robert D.; Kropp, Paul J.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3609 - 3611
反应条件
calcium amide T=120°C;
参考文献
Doklady Akademii Nauk SSSR, , vol. 108, p. 473
Doklady Chemistry, 106-111<1956>273
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 2369,2401;engl.Ausg.S.2458,2462
反应条件
in dichloromethane-d2 T=-70°C; Inert atmosphere; Equilibrium constant;
参考文献
Denmark, Scott E.; Collins, William R.; Cullen, Matthew D.
Journal of the American Chemical Society, 2009 , vol. 131, p. 3490 - 3492
反应条件
ozone in gas T=-40°C; Further byproducts given;
参考文献
Fajgar, Radek; Vitek, Josef; Haas, Yehuda; Pola, Josef
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 2 p. 239 - 248
反应条件
hydrogen; poly-1,2,3-triazolyl ferrocenyl dendrimer-Pd nanoparticle in methanol; chloroform
T=25°C; P=760.051 Torr;
参考文献
Ornelas, Catia; Aranzaes, Jaime Ruiz; Salmon, Lionel; Astruc, Didier
Chemistry - A European Journal, 2008 , vol. 14, # 1 p. 50 - 64
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile
0.75 h; Ambient temperature;
参考文献
Caputo, Romualdo; Mangoni, Lorenzo; Neri, Orsola; Palumbo, Giovanni
Tetrahedron Letters, 1981 , vol. 22, # 36 p. 3551 - 3552
反应条件
benzene cation radical
ΔHo; Thermodynamic data;
参考文献
Meot-Ner, Michael; Pithawalla, Yezdi B.; Gao, Junling; El-Shall, M. Samy
Journal of the American Chemical Society, 1997 , vol. 119, # 35 p. 8332 - 8341
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
1.) 0 deg C, 30 min, 2.) reflux, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Huang, Jiling; Goedken, V.; Walborsky, H. M.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4128 - 4131
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
1.) 0 deg C, 30 min, 2.) reflux, 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Huang, Jiling; Goedken, V.; Walborsky, H. M.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4128 - 4131