1: diphenyl acetylene With anhydrous iron chloride in diethyl ether
T=-78°C; Inert atmosphere;
2: chloro(phenylmethyl)-magnesium in diethyl ether
T=-78 - 12°C; 24 h;
3: With hydrogenchloride; water in diethyl ether
参考文献
Eisch, John J.; Sohn, Jane U.; Rabinowitz, Edon J.
European Journal of Organic Chemistry, 2010 , # 15 p. 2971 - 2977
Van Heerden, Pieter S.; Bezuidenhoudt, Barend C. B.; Ferreira, Daneel
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 8 p. 1141 - 1146
1: in diethyl ether
2.5 h; Heating;
2: With lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether
Heating;
参考文献
Grunewald, Gary L.; Romero, F. Anthony; Chieu, Alex D.; Fincham, Kelcie J.; Bhat, Seema R.; Criscione, Kevin R.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 4 p. 1261 - 1273
