4,4-二甲基-3-氨基硫脲单水合物合成路线 （共 13 条）
反应条件
hydrazine in ethanol T=20°C;
参考文献
WO2009/74157 A1, ;
Page/Page column 74 ;
WO 2009/074157 A1
反应条件
in water 4.5 h; Heating;
参考文献
Mylonas, Stavros; Mamalis, Athanasios
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 7 p. 1273 - 1281
参考文献
Pharmaceutical Chemistry Journal, , vol. 7, # 8 p. 477 - 483
Khimiko-Farmatsevticheskii Zhurnal, , vol. 7, # 8 p. 7 - 13
反应条件
ethanol; hydrazine hydrate
参考文献
Annales de Chimie (Cachan, France), , vol. <12> 7, p. 584,599
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 22, p. 1 - 50
反应条件
in 1,4-dioxane T=80°C; Disproportionation; Cyclization; 1 h; Product distribution; Further Variations:Temperaturesreagent ratio;
参考文献
Russian Chemical Bulletin, , vol. 49, # 2 p. 344 - 347
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , vol. 49, # 2 p. 343 - 346
反应条件
in 1,4-dioxane T=80°C; Disproportionation; Cyclization; 1 h; Product distribution; Further Variations:Temperaturesreagent ratio;
参考文献
Russian Chemical Bulletin, , vol. 49, # 2 p. 344 - 347
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , vol. 49, # 2 p. 343 - 346
反应条件
in 1,4-dioxane T=80°C; Disproportionation; 1 h; Product distribution; Further Variations:Temperaturesreagent ratio;
参考文献
Russian Chemical Bulletin, , vol. 49, # 2 p. 344 - 347
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , vol. 49, # 2 p. 343 - 346
反应条件
triethylamine in N,N-dimethyl-formamide T=20 - 60°C;
参考文献
Su, Xiangdong; Vicker, Nigel; Thomas, Mark P.; Pradaux-Caggiano, Fabienne; Halem, Heather; Culler, Michael D.; Potter, Barry V.L.
ChemMedChem, 2011 , vol. 6, # 8 p. 1439 - 1451
反应条件
sodium chloride in dimethyl sulfoxide
