in tetrahydrofuran; diethyl ether byproducts: C6H5S(O)CH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; reacted for 1 h; not isolated; monitored by (119)Sn NMR spectra; > 95percent conversion;
in tetrahydrofuran; diethyl ether byproducts: Ph2P(O)2CH2MgBr; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in Et2O, SnMe4 (internal standard) and THF mixed; not isolated; monitored by (119)Sn NMR spectra; quantitative conversion;
Moore, M. D.; Lanning, F. C.
Quart. J. Florida Acad. Sci., 1966 , vol. 29, p. 243 - 247
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.1, page 94 - 98
