反应条件
bis(cyclopentadienyl)titanium dichloride in diethyl ether N2-atmosphere; addn. of 5 equiv BuMgBr to precooled GeCl4 soln. (over 1h, stirring, dry ice/Me2CO bath), slow warming to room temp.; addn. of 2 M HCl, extn. of aq. layer (Et2O), drying of org. layer (MgSO4), solvent removal (reduced pressure), filtration, fractional distn. (reduced pressure); elem. anal.;
参考文献
Colacot, Thomas J.
Journal of Organometallic Chemistry, 1999 , vol. 580, # 2 p. 378 - 381
