diethyl ether
Destillation des entstandenen 1-Aethyl-2-butyl-cyclohexanols-(2) in Gegenwart von Jod und anschliessende Hydrierung an Platin in Eisessig unter 2,5 at;
参考文献
Kharasch; Sternfeld
Journal of the American Chemical Society, 1939 , vol. 61, p. 2318,2321
1: n-butyl-magnesium bromide; CH2=CHCH2MgX With manganese (II) chloride in tetrahydrofuran
T=0°C; transmetalation; 0.333333 h;
2: cyclohexenon in tetrahydrofuran
T=-78°C; Addition; dimerization; 0.333333 h;
参考文献
Yorimitsu, Hideki; Hayashi, Yasuhiro; Tang, Jun; Shinokubo, Hiroshi; Oshima, Koichiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 9 p. 2297 - 2300
