water
1.) CH2Cl2, diethyl ether, room temperature, overnight, 2.) diethyl ether, CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shawe, Thomas T.; Hansen, Darren B.; Peet, Kelly Ann; Prokopowicz, Anthony S.; Robinson, Patrice M.; Cannon, Annatina; Dougherty, Kathleen E.; Ross, Andrew A.; Landino, Linda M.
Tetrahedron, 1997 , vol. 53, # 5 p. 1547 - 1556
1: n-butyl-magnesium chloride; 2-Bromobenzoic acid With n-butyllithium
2: 1-Phenylmethyl-piperidin-4-one Reagent/catalystConcentration;
参考文献
Itoh, Takahiro; Kato, Shinji; Nonoyama, Nobuaki; Wada, Toshihiro; Maeda, Kenji; Mase, Toshiaki; Zhao, Matthew M.; Song, Jake Z.; Tschaen, David M.; McNamara, James M.
Organic Process Research and Development, 2006 , vol. 10, # 4 p. 822 - 828
