N,N'-二异丙基碳二亚胺合成路线 （共 71 条）
反应条件
copper(l) chloride 1.) CHCl3, 5 d, r.t.; 2.) CHCl3, 2 d, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tsutsumi, Hideo; Ishido, Yoshiharu
Carbohydrate Research, 1982 , vol. 111, p. 75 - 84
反应条件
1: 23 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 17 h / 140 °C 2: 44 percent / potassium tert-butoxide / dimethylsulfoxide / 7 h / Ambient temperature View Scheme
参考文献
Esser; Pook
Synthesis, 1992 , # 6 p. 596 - 601
反应条件
(i) AcCl, Et2O, (ii) Et3N, N-benzyl-thioacetamide; Multistep reaction;
参考文献
Hartke,K.
Chemische Berichte, 1966 , vol. 99, p. 3163 - 3172
反应条件
in tetrahydrofuran T=75 - 79°C; 1.41667 h; Product distribution / selectivity;
参考文献
Wyeth Holdings Corporation
Patent: US2005/43537 A1, 2005 ;
Location in patent: Page/Page column 5-6 ;
反应条件
copper(l) chloride T=20°C; 24 h;
参考文献
Hodges, John C.; Wang, Wei; Riley, Frank
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2504 - 2508
参考文献
Yu, Yanfei; Li, Zhengning; Jiang, Lan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 632 - 640
反应条件
copper dichloride in acetone
参考文献
Schmidt,E.; Carl,W.
Justus Liebigs Annalen der Chemie, 1961 , vol. 639, p. 24 - 31
反应条件
2-butoxy-ethanol; isopropylamine T=60 - 170°C; 12 h;
参考文献
PPG Industries Ohio, Inc.; Dacko, Christopher; Karabin, Richard F.; Wilson, Craig; Zawacky, Steven R.
Patent: US2013/289272 A1, 2013 ;
Location in patent: Paragraph 0022; 0023 ;
参考文献
Schmidt; Moosmueller
Justus Liebigs Annalen der Chemie, 1955 , vol. 597, p. 235,237
反应条件
silica gel; chromium powder in pentane T=20°C; 15 h;
参考文献
Weiss, Karin; Hoffmann, Kurt
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 6 p. 769 - 773
