1,3-二苯基-2-溴-2-丙烯-1-酮合成路线 (共 26 条)
反应条件
triethylamine in benzene
24 h; Ambient temperature;
参考文献
Rekhter, M. A.; Grushetskaya, G. N.; Panasenko, A. A.; Krimer, M. Z.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 7 p. 792 - 796
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 7 p. 910 - 914
反应条件
1: 78 percent / Br2 / benzene / 2 h / 20 - 25 °C
2: 80 percent / Et3N / benzene / 24 h / Ambient temperature
View Scheme
参考文献
Rekhter, M. A.; Grushetskaya, G. N.; Panasenko, A. A.; Krimer, M. Z.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 7 p. 792 - 796
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 7 p. 910 - 914
反应条件
sodium acetate in ethanol
参考文献
Hortmann,A.G.; Harris,R.L.
Journal of the American Chemical Society, 1971 , vol. 93, p. 2471 - 2481
反应条件
sodium methylate in methanol; dimethyl sulfoxide
T=30°C;
参考文献
Cabaliero, M. C.; Giagante, N. N.
Tetrahedron, 1980 , vol. 36, p. 1829 - 1832
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
0.5 h; Heating;
参考文献
Khurana; Bansal; Chauhan
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 6 p. 1089 - 1091
反应条件
sodium isopropanolate in isopropyl alcohol
T=25°C; kinetic isotope effect; Rate constantMechanism;
参考文献
Cabaleiro, Mercedes C.; Garay, Raul O.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 2 p. 179 - 180
反应条件
sodium methylate in methanol
T=30°C; Rate constantMechanism;
参考文献
Montani, Rosana S.; Garay, Raul O.; Cabaleiro, Mercedes C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1125 - 1130
参考文献
Reynolds
American Chemical Journal, 1910 , vol. 44, p. 321
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Wislicenus,J.; Schmidt
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 226
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Abell
Journal of the Chemical Society, 1912 , vol. 101, p. 1002
反应条件
α-benzylidenacetophenone dibromide;
参考文献
Reynolds
American Chemical Journal, 1910 , vol. 44, p. 321
Full Text Show Details
Wislicenus,J.; Schmidt
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 226
Full Text Show Details
Abell
Journal of the Chemical Society, 1912 , vol. 101, p. 1002
反应条件
1: BrCl / CH2Cl2
2: sodium methoxide / methanol / 30 °C
View Scheme
参考文献
Montani, Rosana S.; Garay, Raul O.; Cabaleiro, Mercedes C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1125 - 1130