四氢-2H-吡喃-2-醇合成路线 (共 136 条)
反应条件
1,1,1-trifluoropropanone; methyl(trifluoromethyl)dioxirane in dichloromethane T=0°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 33, # 29 p. 4225 - 4228
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; (R,S)-binaphos; hydrogen in benzene T=60°C; P=22800 Torr; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 38, # 26 p. 4611 - 4614
反应条件
NiCl2((PPh3)P)2 in toluene
参考文献
Chemical Communications, , # 15 p. 1531 - 1532
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; hydrogen; triphenylphosphine in dichloromethane T=120°C; P=45003.6 Torr; 20 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Organic Letters, , vol. 4, # 2 p. 289 - 291
反应条件
H4Ru4(CO)8lt;P(CH2CH2CH2CH3)3gt;4; hydrogen in diethyl ether; toluene T=200°C; P=98800 Torr; 48 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 109 - 120
反应条件
copper(l) iodide; zinc in water ultrasonic irradiation;
参考文献
Tetrahedron Letters, , vol. 27, # 27 p. 3149 - 3152
反应条件
1: allyl carbinol 0.5 h; Inert atmosphereMolecular sieve; 2: carbon monoxide With dicarbonylacetylacetonato rhodium (I); hydrogen; lithium chloride; (3-butenyloxy)diphenylphosphane in toluene T=40°C; P=15001.5 Torr; 20 h; Molecular sieve; Reactivity; Reagent/catalystSolvent; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 38 p. 7346 - 7349
反应条件
15-crown-5 in sulfolane T=0°C; 1 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 13 p. 3961 - 3970
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 4.5 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187