反应条件
1: 1.) lithium diisopropylamide (LDA) / 1.) THF, from -78 deg C to RT, 2.) THF, reflux, 17.5 h 2: 1.) lithium 2,2,6,6-tetramethylpiperidide, hexamethylphosphoric triamide / 1.) THF, from -78 deg C to RT, 2.) THF, room temp., 30 min 3: 100 percent / acetic acid, 30percent H2O2 / tetrahydrofuran / 0.5 h / 0 °C View Scheme
参考文献
Lane, Kimberley J.; Pinder, A. R.
Journal of Organic Chemistry, 1982 , vol. 47, # 16 p. 3171 - 3172
