苯乙酰胺, N-(1,1-二甲基乙基)-合成路线 (共 21 条)
反应条件
lithium aluminium tetrahydride; diethyl ether; benzene
参考文献
Chiavarelli et al.
Gazzetta Chimica Italiana, 1953 , vol. 83, p. 347,354
反应条件
trifluoroacetic acid Reflux;
参考文献
Chemistry - A European Journal, , vol. 17, # 44 p. 12268 - 12271
反应条件
sulfuric acid in acetic acid
T=20°C; Ritter reaction; 1.5 h; Inert atmosphereEnzymatic reaction;
参考文献
Milne, Jacqueline E.; Baum, Jean C.
Organic Syntheses, 2012 , vol. 89, p. 519 - 526
反应条件
Mg(HSO4)2
T=20°C; 1 h;
参考文献
Salehi; Khodaei; Zolfigol; Keyvan
Synthetic Communications, 2001 , vol. 31, # 13 p. 1947 - 1951
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
4-methyl-morpholine; 2-chloro-4,6-dimethoxy-[1,3,5]triazine in acetonitrile
1 h;
参考文献
Garrett, Christine E.; Jiang, Xinglong; Prasad, Kapa; Repic, Oljan
Tetrahedron Letters, 2002 , vol. 43, # 23 p. 4161 - 4165
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in acetonitrile
T=60°C; 10 h; Inert atmosphere;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271
反应条件
N-iodo-succinimide; water; potassium carbonate in tetrahydrofuran
T=0°C;
参考文献
Shen, Bo; Makley, Dawn M.; Johnston, Jeffrey N.
Nature, 2010 , vol. 465, # 7301 p. 1027 - 1032
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=110°C; P=15514.9 Torr; 15 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in acetonitrile
T=60°C; 10 h; Inert atmosphere;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271