(3,3-二乙氧基丙基)苯合成路线 (共 20 条)
反应条件
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone in acetonitrile 5 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 14 p. 979 - 980
反应条件
pyridinium p-toluenesulfonate in acetone 5 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 109, # 23 p. 7122 - 7127
反应条件
pyridinium p-toluenesulfonate in acetone 5 h; Heating;
参考文献
Parrinello, Giovanni; Stille, J. K.
Journal of the American Chemical Society, 1987 , vol. 109, # 23 p. 7122 - 7127
反应条件
sodium hypochlorite in acetic acid; acetone T=0°C; 5 h;
参考文献
Sugai, Saburo; Kodama, Takashi; Akaboshi, Sanya; Ikegami, Shiro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 99 - 105
反应条件
gallium(III) iodide in ethanol
T=20°C; 1.33333 h; Inert atmosphere;
参考文献
Ding, Jin-Chang; Xu, Rong; Liu, Miao-Chang; Chen, Xi-An; Wu, Hua-Yue
Journal of the Indian Chemical Society, 2008 , vol. 85, # 5 p. 566 - 568
反应条件
1-methyl-pyrrolidin-2-one; palladium diacetate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20°C; Kumada coupling; 20 h;
参考文献
Frisch, Anja C.; Shaikh, Nadim; Zapf, Alexander; Belier, Matthias
Angewandte Chemie - International Edition, 2002 , vol. 41, # 21 p. 4056 - 4059
反应条件
hydrogen; tin(ll) chloride; ((2S,4S)-N-(tert-butoxycarbonyl)-4-(diphenylphosphino)-2-{(diphenylphosphino)methyl}pyrrolidine)PtCl2
T=60°C; P=139630 Torr; 150 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Parrinello, Giovanni; Stille, J. K.
Journal of the American Chemical Society, 1987 , vol. 109, # 23 p. 7122 - 7127
反应条件
N-chloro-succinimide; thiourea
T=23°C; 0.25 h;
参考文献
Mei; Bentley; Du
Tetrahedron Letters, 2009 , vol. 50, # 29 p. 4199 - 4200
反应条件
hydrogen; Au colloid
T=79.84°C; P=15001.5 Torr;
参考文献
Parvulescu, Vasile I.; Parvulescu, Viorica; Endruschat, Uwe; Filoti, George; Wagner, Friedrich E.; Kuebel, Christian; Richards, Ryan
Chemistry - A European Journal, 2006 , vol. 12, # 8 p. 2343 - 2357
反应条件
toluene-4-sulfonic acid
2 h;
参考文献
Padwa, Albert; Bullock, William H.; Dyszlewski, Andrew D.; McCombie, S. W.; Shankar, B. B.; Ganguly, A. K.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3556 - 3564