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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苯甲醚
合成路线
（共 1687 条）
402-50-6
4-(三氟甲基)苯乙烯
+
696-62-8
4-碘苯甲醚
→
反应条件
68036-77-1
+
40473-89-0
反应条件
in N,N-dimethyl-formamide; toluene T=120°C; Heck Reaction; 0.833333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
288-88-0
1,2,4-三氮唑
+
696-62-8
4-碘苯甲醚
→
反应条件
68377-33-3
1-(4-甲氧基苯基)-1H-1,2,4-三唑
反应条件
copper(l) iodide; 2-methyl-8-hydroxyquinoline; potassium carbonate in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Zhang, Yihua; Yang, Xinye; Xing, Hui; Zhang, Ye; Lai, Yisheng; Jiang, Yongwen; Ma, Dawei
Chinese Journal of Chemistry, 2012 , vol. 30, # 4 p. 875 - 880
696-62-8
4-碘苯甲醚
+
1666-13-3
二苯基二硒醚
→
反应条件
80448-01-7
反应条件
copper(l) iodide; caesium carbonate in acetonitrile T=82°C; 28 h; Inert atmosphere;
参考文献
Dandapat, Arpan; Korupalli, Chiranjeevi; Prasad; Singh, Rahul; Sekar, Govindasamy
Synthesis, 2011 , # 14 art. no. Z31111SS, p. 2297 - 2302
696-62-8
4-碘苯甲醚
+
41924-21-4
→
反应条件
80448-01-7
反应条件
tetrakis(triphenylphosphine) palladium(0); 1-n-butyl-3-methylimidazolium hexafluorophosphate T=80°C; 4 h; Inert atmosphere;
参考文献
Zhao, Hong; Hao, Wenyan; Xi, Zhiwen; Cai, Mingzhong
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2661 - 2665
696-62-8
4-碘苯甲醚
+
645-96-5
苯硒酚
→
反应条件
80448-01-7
反应条件
copper(l) iodide; 2,9-dimethyl-1,10-phenanthroline; sodium t-butanolate in toluene T=110°C; 24 h;
参考文献
Gujadhur, Rattan K.; Venkataraman
Tetrahedron Letters, 2003 , vol. 44, # 1 p. 81 - 84
696-62-8
4-碘苯甲醚
+
14971-39-2
→
反应条件
22216-66-6
+
1132-39-4
二苯硒醚
+
80448-01-7
反应条件
in ammonia 4.33333 h; Irradiation;
参考文献
Pierini, Adriana B.; Penenory, Alicia B.; Rossi, Roberto A.
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 486 - 490
1514-82-5
2-溴-3,3,3-三氟丙烯
+
696-62-8
4-碘苯甲醚
→
反应条件
82203-83-6
反应条件
1: 2-Bromo-3,3,3-trifluoro-propene With ZnCl2*TMEDA; lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 2: para-iodoanisole With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane 6 h; Heating;
参考文献
Konno, Tsutomu; Chae, Jungha; Kanda, Masashi; Nagai, Go; Tamura, Kazushige; Ishihara, Takashi; Yamanaka, Hiroki
Tetrahedron, 2003 , vol. 59, # 38 p. 7571 - 7580
6165-69-1
3-噻吩硼酸
+
696-62-8
4-碘苯甲醚
→
反应条件
82437-75-0
反应条件
water; triethylamine; Pd(OAc)2EnCatTM in N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura reaction; 0.25 h; microwave irradiation;
参考文献
Vickerstaffe, Emma; Villard, Anne-Laure; Ladlow, Mark; Ley, Steven V.
Synlett, 2007 , # 8 p. 1251 - 1254
872-31-1
3-溴噻吩
+
696-62-8
4-碘苯甲醚
→
反应条件
82437-75-0
反应条件
PEG 4000; palladium diacetate; potassium carbonate T=120°C; 10 h;
参考文献
Wang, Liang; Zhang, Yuhong; Liu, Leifang; Wang, Yanguang
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1284 - 1287
188290-36-0
+
696-62-8
4-碘苯甲醚
→
反应条件
82437-75-0
+
42545-43-7
2-(4-甲氧苯基)噻吩
反应条件
potassium tert-butylate in dimethyl sulfoxide T=20°C; 3 h; Schlenk techniqueInert atmosphereIrradiation; TimeTemperatureConcentrationReagent/catalyst; Overall yield = 90 percent;
参考文献
Buden, Maria E.; Guastavino, Javier F.; Rossi, Roberto A.
Organic Letters, 2013 , vol. 15, # 6 p. 1174 - 1177
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