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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
69622-35-1
合成路线
（共 11 条）
120-72-9
吲哚
+
3282-30-2
三甲基乙酰氯
→
反应条件
69622-35-1
反应条件
1: indole With diethylaluminium chloride in hexane; dichloromethane T=0°C; 0.5 h; 2: pivaloyl chloride in hexane; dichloromethane T=0°C; 2 h; Further stages.;
参考文献
Liu, Songbai; Liebeskind, Lanny S.
Journal of the American Chemical Society, 2008 , vol. 130, # 22 p. 6918 - 6919
120-72-9
吲哚
+
815-17-8
三甲基丙酮酸
→
反应条件
69622-35-1
反应条件
iodine; oxygen; palladium diacetate; caesium carbonate in 1-methyl-pyrrolidin-2-one T=45°C; 12 h; Schlenk techniqueSealed tube;
参考文献
Gu, Li-Jun; Liu, Ji-Yan; Zhang, Li-Zhu; Xiong, Yong; Wang, Rui
Chinese Chemical Letters, 2014 , vol. 25, # 1 p. 90 - 92
111122-97-5
→
反应条件
69622-35-1
反应条件
tetrafluoroboric acid; mercury(II) oxide in tetrahydrofuran Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
105399-11-9
→
反应条件
69622-35-1
反应条件
copper (II) chromite in quinoline
参考文献
Murakami; Tani; Suzuki; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4707 - 4716
120-72-9
吲哚
→
反应条件
69622-35-1
反应条件
1: 90 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature 2: 100 percent / HgO, 35percent aq. tetrafluoroboric acid / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
59045-53-3
→
反应条件
69622-35-1
反应条件
1: 90 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature 2: 100 percent / HgO, 35percent aq. tetrafluoroboric acid / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
69622-35-1
反应条件
1: tetrafluoroboric acid/ether complex / acetonitrile 2: 90 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature 3: 100 percent / HgO, 35percent aq. tetrafluoroboric acid / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
3770-50-1
吲哚-2-羧酸乙酯
→
反应条件
69622-35-1
反应条件
1: 93.2 percent / trifluoroacetic anhydride, 85 percent phosphoric acid / acetonitrile / 1 h / Ambient temperature 2: 94.3 percent / KOH / ethanol / Heating 3: 87.8 percent / copper chromite / quinoline View Scheme
参考文献
Murakami; Tani; Suzuki; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4707 - 4716
77069-12-6
→
反应条件
69622-35-1
反应条件
1: 94.3 percent / KOH / ethanol / Heating 2: 87.8 percent / copper chromite / quinoline View Scheme
参考文献
Murakami; Tani; Suzuki; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4707 - 4716
75-98-9
特戊酸
→
反应条件
69622-35-1
反应条件
1: 93.2 percent / trifluoroacetic anhydride, 85 percent phosphoric acid / acetonitrile / 1 h / Ambient temperature 2: 94.3 percent / KOH / ethanol / Heating 3: 87.8 percent / copper chromite / quinoline View Scheme
参考文献
Murakami; Tani; Suzuki; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 11 p. 4707 - 4716
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