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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6963-45-7
合成路线
（共 23 条）
1123-34-8
1-烯丙基环己醇
→
反应条件
6963-45-7
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C; 10 h;
参考文献
Shao, Zhi-Hui; Peng, Fang-Zhi; Chen, Jing-Bo; Wang, Chen-Ying; Huang, Rong; Tu, Yong-Qiang; Li, Liang; Zhang, Hong-Bin
Synthetic Communications, 2004 , vol. 34, # 11 p. 2031 - 2038
109-72-8
正丁基锂
+
627-32-7
3-碘丙醇
+
108-94-1
环己酮
→
反应条件
5445-30-7
1-正-丁基环己醇
+
6963-45-7
反应条件
1: 3-iodo-prop-2 (Z)-ene-ol With isopropylmagnesium chloride in tetrahydrofuran T=-78°C; 0.0833333 h; 2: n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.333333 h; 3: cyclohexanone in tetrahydrofuran; hexane T=-78°C; 0.5 h; Further stages.;
参考文献
Fleming, Fraser F.; Gudipati, Subrahmanyam; Vu, Viet Anh; Mycka, Robert J.; Knochel, Paul
Organic Letters, 2007 , vol. 9, # 22 p. 4507 - 4509
3384-04-1
+
108-94-1
环己酮
→
反应条件
6963-45-7
反应条件
1: 3-chloropropyl phenyl ether With di(tert-butyl)-biphenyl; lithium in tetrahydrofuran T=-78°C; Metallation; 0.5 h; 2: cyclohexanone T=20°C; Addition; 1.5 h; 3: cyclohexanone T=-78°C; Addition; 0.0833333 h; Further stages.;
参考文献
Foubelo, Francisco; Saleh, Sadiq A.; Yus, Miguel
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3478 - 3483
699-61-6
1-羟基环己烷丙酸 gamma-内酯
→
反应条件
6963-45-7
反应条件
lithium borohydride in tetrahydrofuran 36 h; Ambient temperature;
参考文献
Alonso, Daniel; Font, Josep; Ortuno, Rosa M.
Journal of Organic Chemistry, 1991 , vol. 56, # 19 p. 5567 - 5572
3384-04-1
+
108-94-1
环己酮
+
630-19-3
特戊醛
→
反应条件
6963-45-7
反应条件
1: 3-chloropropyl phenyl ether With di(tert-butyl)-biphenyl; lithium in tetrahydrofuran T=-78°C; Metallation; 0.5 h; 2: cyclohexanone T=20°C; Addition; 1.5 h; 3: pivalaldehyde T=-78°C; Addition; 0.0833333 h; Further stages.;
参考文献
Foubelo, Francisco; Saleh, Sadiq A.; Yus, Miguel
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3478 - 3483
3384-04-1
+
108-94-1
环己酮
+
100-52-7
苯甲醛
→
反应条件
6963-45-7
反应条件
1: 3-chloropropyl phenyl ether With di(tert-butyl)-biphenyl; lithium in tetrahydrofuran T=-78°C; Metallation; 0.5 h; 2: cyclohexanone T=20°C; Addition; 1.5 h; 3: benzaldehyde T=-78°C; Addition; 0.0833333 h; Further stages.;
参考文献
Foubelo, Francisco; Saleh, Sadiq A.; Yus, Miguel
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3478 - 3483
3384-04-1
+
108-94-1
环己酮
+
107-87-9
2-戊酮
→
反应条件
6963-45-7
反应条件
1: 3-chloropropyl phenyl ether With di(tert-butyl)-biphenyl; lithium in tetrahydrofuran T=-78°C; Metallation; 0.5 h; 2: cyclohexanone T=20°C; Addition; 1.5 h; 3: pentan-2-one T=-78°C; Addition; 0.0833333 h; Further stages.;
参考文献
Foubelo, Francisco; Saleh, Sadiq A.; Yus, Miguel
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3478 - 3483
3384-04-1
+
10458-14-7
5-甲基-2-异丙基环己酮
+
108-94-1
环己酮
→
反应条件
6963-45-7
反应条件
1: 3-chloropropyl phenyl ether With di(tert-butyl)-biphenyl; lithium in tetrahydrofuran T=-78°C; Metallation; 0.5 h; 2: cyclohexanone T=20°C; Addition; 1.5 h; 3: (-)-Menthone T=-78°C; Addition; 0.0833333 h; Further stages.;
参考文献
Foubelo, Francisco; Saleh, Sadiq A.; Yus, Miguel
Journal of Organic Chemistry, 2000 , vol. 65, # 11 p. 3478 - 3483
108-28-1
原白头翁素
→
反应条件
6963-45-7
反应条件
1: 85 percent / hydroquinone / 4 h / 155 °C 2: 87 percent / H2 / 10percent Pd/C / 760 - 1520 Torr / Ambient temperature 3: 85 percent / LiBH4 / tetrahydrofuran / 36 h / Ambient temperature View Scheme
参考文献
Alonso, Daniel; Font, Josep; Ortuno, Rosa M.
Journal of Organic Chemistry, 1991 , vol. 56, # 19 p. 5567 - 5572
84477-25-8
→
反应条件
6963-45-7
反应条件
1: 87 percent / H2 / 10percent Pd/C / 760 - 1520 Torr / Ambient temperature 2: 85 percent / LiBH4 / tetrahydrofuran / 36 h / Ambient temperature View Scheme
参考文献
Alonso, Daniel; Font, Josep; Ortuno, Rosa M.
Journal of Organic Chemistry, 1991 , vol. 56, # 19 p. 5567 - 5572
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