2-氯-2,6-二乙基乙酰苯胺合成路线 (共 11 条)
反应条件
in ethyl acetate Acylation; 2 h; Heating;
参考文献
Nesnow, Stephen; Agarwal, Satish C.; Padgett, William T.; Lambert, Guy R.; Boone, Phillip; Richard, Ann M.
Chemical Research in Toxicology, 1995 , vol. 8, # 2 p. 209 - 217
反应条件
methyl lithium LiBr complex in diethyl ether T=-78°C;
参考文献
Pace, Vittorio; Castoldi, Laura; Holzer, Wolfgang
Chemical Communications, 2013 , vol. 49, # 75 p. 8383 - 8385
反应条件
hydrogenchloride in acetone Hydrolysis; 4 h; Heating;
参考文献
Environmental Science and Technology, , vol. 29, # 6 p. 1557 - 1563
反应条件
sodium iodide in acetone 10 h; Heating;
参考文献
Dumitrascu, Florea; Mitan, Carmen Irena; Draghici, Constantin; Caproiu, Miron Teodor; Caprau, Delia; Dumitrescu, Denisa
Revue Roumaine de Chimie, 2002 , vol. 47, # 3-4 p. 309 - 314
反应条件
sodium hydroxide; PEG-400 in benzene T=15°C; 2 h; Yield given;
参考文献
Zupancic, Boris G.; Sopcic, Mirko
Synthesis, 1982 , # 11 p. 942 - 944
反应条件
sodium hydroxide; PEG-400 in benzene T=15°C; 2 h; Yield given;
参考文献
Zupancic, Boris G.; Sopcic, Mirko
Synthesis, 1982 , # 11 p. 942 - 944
反应条件
sodium hydroxide; PEG-400 in benzene T=15°C; 2 h; Yield given;
参考文献
Zupancic, Boris G.; Sopcic, Mirko
Synthesis, 1982 , # 11 p. 942 - 944
反应条件
toluene-4-sulfonic acid 5 h; Heating;
参考文献
Ledneczki, Istvan; Agocs, Pal M.; Molnar, Arpad
Synlett, 2003 , # 14 p. 2255 - 2257
反应条件
sodium hydroxide; PEG-400 in benzene
T=15°C; 2 h; Yield given;
参考文献
Zupancic, Boris G.; Sopcic, Mirko
Synthesis, 1982 , # 11 p. 942 - 944
反应条件
sodium sulfate; paraformaldehyde in Petroleum ether; benzene
参考文献
PPG Industries, Inc.
Patent: US4319917 A1, 1982 ;