四氟乙烷-beta-磺内酯合成路线 （共 50 条）
参考文献
Chen, Zili; Xiong, Wennan; Jiang, Biao
Chemical Communications, 2002 , # 18 p. 2098 - 2099
反应条件
in neat (no solvent) at 5°C, with polytetrafluoroethylene filled reactor used; distn.;
参考文献
Dmitriev, M. A.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 966 - 969
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1035 - 1038
C.A., 1960 , p. 24341
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
NAF 1.) room temperature, 6 days; 2.) 40-50 deg C, 18 days;
参考文献
Terjeson, Robin J.; Mohtasham, Javid; Sheets, Roger M.; Gard, Gary L.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 3 - 18
反应条件
warming on water bath under reflux, at 50-60°C, 4 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
silver fluoride
1.) diglyme, -196 deg C, then 1 h at room temp.; 2.) -196 deg C, then 12 h at 30-40 deg C; Yield given. Multistep reaction;
参考文献
Chen, L. F.; Mohtasham, J.; Gard, G. L.
Journal of Fluorine Chemistry, 1990 , vol. 46, # 1 p. 21 - 38
反应条件
in dichloromethane
at -10°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
