4’,5’-二甲基-2’-硝基乙酰苯胺合成路线 （共 15 条）
反应条件
sulfuric acid; nitric acid in acetic acid T=20°C; 0.5 h;
参考文献
Chattopadhyay, Prosenjit; Nagpal, Rekha; Pandey, Pramod S.
Australian Journal of Chemistry, 2008 , vol. 61, # 3 p. 216 - 222
反应条件
acetic acid Acetylation; 1 h; Heating;
参考文献
Kojima, Hirotatsu; Nakatsubo, Naoki; Kikuchi, Kazuya; Kawahara, Shigenori; Kirino, Yutaka; Nagoshi, Hiroshi; Hirata, Yasunobu; Nagano, Tetsuo
Analytical Chemistry, 1998 , vol. 70, # 13 p. 2446 - 2453
反应条件
1: acetic acid; H2O / 1 h / 60 °C 2: 70 percent aq. HNO3, AcOH / 1 h / below 15 deg C View Scheme
参考文献
Synthesis, , # 10 p. 1257 - 1262
反应条件
1: polyphosphoric acid; NH2OH+HCl 2: acetic acid; Cu(NO3)2 View Scheme
参考文献
Yakugaku Zasshi, , vol. 75, p. 881
Chem.Abstr., , p. 4920
反应条件
copper(II) nitrate; acetic acid
参考文献
Yakugaku Zasshi, , vol. 75, p. 881
Chem.Abstr., , p. 4920
反应条件
copper(II) nitrate; acetic acid
参考文献
Yakugaku Zasshi, , vol. 75, p. 881
Chem.Abstr., , p. 4920
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 68, p. 88,89
反应条件
1: 97.4 percent / conc. HCl / 100 °C 2: 40 g / hydrogene / 2percent Pd/C / aq. ethanol / 2 h / 30 - 60 °C / 44133.5 Torr View Scheme
参考文献
Maslennikova, T. A.; Shaburov, V. V.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 1 p. 134 - 146,119 - 128
反应条件
1: NBS, (PhCO)2O2 / CCl4 2: CaCO3 / H2O 3: aq. KOH 4: (i) isopentyl nitrite, HCl, EtOH, (ii) H2SO4, aq. EtOH View Scheme
参考文献
Die Pharmazie, , vol. 24, # 2 p. 87 - 94
反应条件
1: picric acid; boric acid; iron (II)-sulfate / und konz. Schwefelsaeure 2: SnCl2; aqueous HCl 3: ethanol; aqueous sodium nitrite; sulfuric acid / Diazotization.Erwaermen der Diazoniumsalz-Loesung View Scheme
参考文献
Manske et al.
Canadian Journal of Research, Section B: Chemical Sciences, 1942 , vol. 20, p. 133,135
