(2E)-2-(二氢-2(3H)-呋喃亚基)-1-苯基-乙酮合成路线 （共 5 条）
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=68°C; 2 h;
参考文献
Bellur, Esen; Langer, Peter
Tetrahedron, 2006 , vol. 62, # 23 p. 5426 - 5434
反应条件
aluminium trichloride; potassium chloride in dichloromethane
0.5 h;
参考文献
De, Dibyendu; Seth, M.; Bhaduri, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 503 - 506
反应条件
water; acetic acid
T=70°C; 1 h;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Cimarelli, Cristina; Dalpozzo, Renato; Palmieri, Gianni
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 16 p. 2095 - 2100
反应条件
1: 80 percent / sodium methoxide / benzene / 4 h / Ambient temperature; 4 moles of NaOMe
2: 70 percent / AlCl3, KCl / CH2Cl2 / 0.5 h
View Scheme
参考文献
De, Dibyendu; Seth, M.; Bhaduri, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 503 - 506
反应条件
1: 1) MeLi, TMEDA / 1) THF, a) 0 to 20 deg C, b) 2 h, 20 deg C, 2) THF, a) -50 deg C to r.t., b) r.t.
2: 68 percent / AcOH, water / 1 h / 70 °C
View Scheme
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Cimarelli, Cristina; Dalpozzo, Renato; Palmieri, Gianni
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 16 p. 2095 - 2100
