6-氯-1,3-二甲基脲嘧啶合成路线 (共 66 条)
反应条件
sodium azide in ethanol
Substitution; 2 h; Heating;
参考文献
Bhuyan, Pulak J.; Borah, Harsha N.; Sandhu, Jagir S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 21 p. 3083 - 3084
参考文献
Pfleiderer; Ferch
Justus Liebigs Annalen der Chemie, 1958 , vol. 615, p. 52,55
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water
2 h; Ambient temperature;
参考文献
Gogoi, Mukti; Sandhu, Jagir S.; Baruah, J. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 851 - 852
反应条件
in methanol
T=60°C; 0.00833333 h; microwave irradiation;
参考文献
Fang, Woei-Ping; Cheng, Yuh-Tsyr; Cheng, Yann-Ru; Cherng, Yie-Jia
Tetrahedron, 2005 , vol. 61, # 12 p. 3107 - 3113
反应条件
in methanol
T=20°C; 1 h; UV-irradiation;
参考文献
Ohkura, Kazue; Uchiyama, Shun; Aizawa, Kazuya; Nishijima, Ken-Ichi; Seki, Koh-Ichi
Heterocycles, 2002 , vol. 57, # 8 p. 1403 - 1408
反应条件
1: NaOH / ethanol; H2O
2: 58 percent / acetonitrile / 4 h / Irradiation
View Scheme
参考文献
Edstrom, Eric D.; Yuan, Wei
Tetrahedron Letters, 1991 , vol. 32, # 3 p. 323 - 326