反应条件
di-tert-butyl peroxide in neat (no solvent) addn. of peroxide to equimolar mixt. of (CH2CHCH2)4Sn and PhCHOCH2, 24h, 130°C, acidolysis by addn. of malonic acid in ether, reflux, 48h, ether removed, pptn. of malonate by addn. of pentane, under Ar; alcohol detected by chromy., total yield: 34percent;
参考文献
Journal of Organometallic Chemistry, , vol. 190, # 1 p. 43 - 52