5-(氯代磺酰基)-2-糠酸甲酯合成路线 （共 5 条）
反应条件
phosphorus pentachloride T=150°C; 3 h;
参考文献
WO2007/60215 A2, ;
Page/Page column 15 ;
反应条件
1: chlorosulfonic acid / CHCl3 / 3 h / 50 °C 2: 1.) 15percent aq. KOH, 2.) PCl5 3: 0.5 h / 40 °C View Scheme
参考文献
Pharmaceutical Chemistry Journal, , vol. 17, # 6 p. 410 - 414
Khimiko-Farmatsevticheskii Zhurnal, , vol. 17, # 6 p. 685 - 688
反应条件
1: 1.) 15percent aq. KOH, 2.) PCl5 2: 0.5 h / 40 °C View Scheme
参考文献
Pharmaceutical Chemistry Journal, , vol. 17, # 6 p. 410 - 414
Khimiko-Farmatsevticheskii Zhurnal, , vol. 17, # 6 p. 685 - 688
反应条件
T=40°C; 0.5 h; Yield given;
参考文献
Pharmaceutical Chemistry Journal, , vol. 17, # 6 p. 410 - 414
Khimiko-Farmatsevticheskii Zhurnal, , vol. 17, # 6 p. 685 - 688
反应条件
ammonia in diethyl ether
参考文献
Abovyan, L. S.; Shkulev, V. A.; Stepanyan, N. O.; Agaronyan, A. S.; Mndzhoyan, O. L.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 6 p. 410 - 414
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 6 p. 685 - 688
