4-甲氧基-1,2-苯醌合成路线 （共 12 条）
反应条件
potassium dihydrogenphosphate; K4(ON(SO3)2)2 in water
T=5°C; 1 h;
参考文献
Carlson, Brian W.; Miller, Larry L.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 479 - 485
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in DMF-d7
T=25°C; 8 h;
参考文献
Magdziak, Derek; Rodriguez, Andy A.; Van De Water, Ryan W.; Pettus, Thomas R. R.
Organic Letters, 2002 , vol. 4, # 2 p. 285 - 288
反应条件
diethyl ether; sodium sulfate; silver(l) oxide
参考文献
Kvalnes
Journal of the American Chemical Society, 1934 , vol. 56, p. 2487
反应条件
1: 75 percent / boric acid; aq. H2O2; aq. H2SO4 / tetrahydrofuran / 12 h / 20 °C
2: 67 percent / potassium carbonate / acetone / 6 h / Heating
3: 77 percent / H2 / Pd/C / atmospheric pressure
4: 2,2-diphenyl-1-picrylhydrazyl / tetradeuteriomethanol; acetone-d6 / 0.17 h
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: 67 percent / potassium carbonate / acetone / 6 h / Heating
2: 77 percent / H2 / Pd/C / atmospheric pressure
3: 2,2-diphenyl-1-picrylhydrazyl / tetradeuteriomethanol; acetone-d6 / 0.17 h
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: 77 percent / H2 / Pd/C / atmospheric pressure
2: 2,2-diphenyl-1-picrylhydrazyl / tetradeuteriomethanol; acetone-d6 / 0.17 h
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: 84 percent / potassium carbonate / acetone / 4 h / Heating
2: 75 percent / boric acid; aq. H2O2; aq. H2SO4 / tetrahydrofuran / 12 h / 20 °C
3: 67 percent / potassium carbonate / acetone / 6 h / Heating
4: 77 percent / H2 / Pd/C / atmospheric pressure
5: 2,2-diphenyl-1-picrylhydrazyl / tetradeuteriomethanol; acetone-d6 / 0.17 h
View Scheme
参考文献
Saito, Shizuka; Kawabata, Jun
Tetrahedron, 2005 , vol. 61, # 34 p. 8101 - 8108
反应条件
1: aqueous NaOH; aqueous H2O2
2: Ag2O; Na2SO4; diethyl ether
View Scheme
参考文献
Kvalnes
Journal of the American Chemical Society, 1934 , vol. 56, p. 2487
反应条件
chromium(VI) oxide in water
T=25°C; Oxidation; pH=5; Kinetics; Further Variations:pH-values;
参考文献
Elovitz, Michael S.; Fish, William
Environmental Science & Technology, 1995 , vol. 29, # 8 p. 1933 - 1943
反应条件
periodate(1-) in acetic acid
T=25°C; Rate constantMechanism;
参考文献
Srivastava; Bhattacharjee; Malik
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 347 - 348
