2-甲氧基-3,5-二甲基环戊-2-烯-1-酮合成路线 （共 4 条）
参考文献
Givaudan Corporation
Patent: US4892966 A1, 1990 ;
反应条件
1: acetyl chloride
2: sodium hydride / diethyl ether; paraffin / Heating
3: tetrabutylammonium hydrogen sulfate, aq. sodium hydroxide / CH2Cl2 / 0.33 h
View Scheme
参考文献
Arnarp, Jan; Enzell, Curt; Petersson, Kurt; Pettersson, Tore
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 839 - 854
反应条件
1: sodium hydride / diethyl ether; paraffin / Heating
2: tetrabutylammonium hydrogen sulfate, aq. sodium hydroxide / CH2Cl2 / 0.33 h
View Scheme
参考文献
Arnarp, Jan; Enzell, Curt; Petersson, Kurt; Pettersson, Tore
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 839 - 854
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane
0.333333 h; Yield given;
参考文献
Arnarp, Jan; Enzell, Curt; Petersson, Kurt; Pettersson, Tore
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 839 - 854
